Mechanical Properties of 3D-Printed Denture Base Materials Under Biomimetic Conditions
Objectives: To compare flexural strength, fracture toughness, and creep properties of four 3D-printed denture base materials under biomimetic conditions. Methods: Four commercially available 3D-printed denture base materials, Formlabs-Denture-Base-OP, Pacdent-Denture-Base, Lucitone-Digital-Print, and DENTCA-Denture-Base-II, were used in the study. Rectangular bar-shaped specimens were designed and printed with DLP-3D-printing machine and post-processed according to the manufacturer's instructions. Twenty-sixth specimens for each material were printed. Single-edge notched bars of 3x4x25mm3 were used for fracture toughness test(n=9); 4x8x40mm3 for three-point-bend flexural strength test(n=10), and 3x9x50mm3 for creep compliance test(n=6).
Specimens were tested at a controlled temperature 37±2°C using an environmental control chamber under an Instron-Universal-Testing-Machine. Three-point-bend was tested 1mm/min crosshead-speed and 20-mm-span until fracture. Specimens for fracture toughness were inspected under an optical-microscope for crack length and tested failure load using three-point-bend fixture with support 20-mm, crosshead-speed 0.5mm/min. Six specimens were used for creep test by loading specimens with displacement 1mm/min crosshead speed and holding 70%(20% for Lucitone) of mean failure stress 10minutes. All values were calculated using one-way-ANOVA. The levels were compared by Tukey-KramerHSD using JMP-Pro16.2. Results: DENTCA-Denture-Base-II and Formlabs-Denture-Base-OP showed significantly higher flexural strength than Lucitone-Digital-Print and Pacdent-Denture-Base,P<0.0001. However, Lucitone-Digital-Print had fracture toughness significantly higher than DENTCA-Denture-Base-II, Formlabs-Denture-Base-OP,and Pacdent-Denture-Base, respectively,P<0.0001. Lucitone-Digital-Print showed a significantly higher creep compliance percentage than Pacdent-Denture-Base, DENTCA-Denture-Base-II, and Formlabs-Denture-Base-OP,P<0.0001. Conclusions: DENTCA-Denture-Base-II and Formlabs-Denture-Base-OP exhibit higher flexural strength than Lucitone-Digital-Print and Pacdent-Denture-Base.However, Lucitone-Digital-Print demonstrates superior fracture toughness compared to other materials.Regarding creep compliance, Lucitone-Digital-Print shows the highest percentage, indicating greater susceptibility to time-dependent deformation.
2023 South East Asian Division Meeting (Singapore) Singapore
2023 029 Dental Materials 2: Polymer-based Materials
Choochaisaengrat, Setthawut
( Boston Univerisity
, Boston
, Massachusetts
, United States
)
Lubell, Aaron
( Boston Univerisity
, Boston
, Massachusetts
, United States
)
Zhao, Minglei
( Boston Univerisity
, Boston
, Massachusetts
, United States
)
Giordano Ii, Russell
( Boston Univerisity
, Boston
, Massachusetts
, United States
)
Fan, Yuwei
( Boston Univerisity
, Boston
, Massachusetts
, United States
)
The mean and standard deviation of three-point flexural strength, fracture toughness and Creep compliance percentage of four 3D-printed denture base materials.
3D Printed Material
3 Point Flexural Strength (MPa)
Fracture toughness (MPa-m½)
Creep Compliance, %
N
Mean
Std Dev
CV
Sig level*
N
Mean
Std Dev
CV
Sig level*
N
Mean Percentage
Std Dev Percentage
CV
Sig level*
DENTCA Denture-Base-II
10
99.22
6.34
6.39
A
9
1.25
0.09
7.28
B
6
58.67
18.79
32.03
C
Formlabs Denture-Base-OP
10
96.32
4.04
4.19
A
9
0.61
0.07
12.02
C
6
18.32
2.03
11.09
D
Lucitone Digital-Print
10
47.41
1.94
4.10
B
9
2.37
0.50
21.22
A
6
314
9.50
3.04
A
Pacdent Denture-Base
10
44.57
1.84
4.12
B
9
0.56
0.10
17.18
C
6
87.67
12.01
13.70
B
*Levels not connected by the same letter are significantly different.