Objective: To evaluate bonding durability of two all-in-one adhesive systems to dentin after long-term storage in water. Material and Method: Flat coronal dentin surfaces of extracted human molars were prepared, leaving the surrounding enamel. Two all-in-one adhesive systems: Tri-S Bond (Kuraray Medical Co.) and G-Bond (GC Co.), were applied to both dentin and the surrounding enamel surfaces according to manufacturer's instructions. Following resin composite (Clearfil AP-X) buildups, the bonded specimens were stored in 37 oC water for 24 hours (control group), 3 and 6 months. After the designated periods of water storage, the specimens were serially sectioned perpendicular to the adhesive interface into 0.7 mm thick slabs, and then trimmed to form hour-glass configurations with a 1 mm2 cross-sectional area. The micro-tensile bond strength (mTBS) test was carried out at a crosshead speed of 1.0 mm/min. The data were statistically analyzed using two-way ANOVA and T-test (P<0.05).
Results: Two-way ANOVA revealed that there was significant difference between materials, but not significant difference between storage periods.
|
|
Control(24 hours) |
3 months |
6 months |
|
Tri-S Bond |
44.4(7.7)a |
43.2(4.9) b |
44.8(10.7)c |
|
G-Bond |
39.4(9.1) a |
37.5(9.1) b |
38.4(6.6) c |
mean bond strength(SD)(MPa, n=10). Same letter within the vertical rows indicates that there were no significant differences as tested by T-test (P<0.05).
Conclusion: For both adhesive systems, the mTBS to dentin were almost stable during 6 months water storage when the surrounding enamel was present.