Mechanical properties of the bonded interface and those of the surface dentin layer in which the bonded procedure is produced, affect attained bond strength. Objectives: The aim is to determine if primary dentin microhardness (MH) is affected by different chemical dentin pre-treatments performed for resin bonding. Methods: Dentin discs were obtained by transversally sectioning the crowns of human primary first molars. Knoop MH was measured after different treatments: (1) polished up to 4000 grit, (2) polished and etched (37% ortophosphoric acid) for 7s or 15 s, (3) polished, etched for 7s or 15 s and treated with 5% NaOCl for 2 min. Indentations (n=20) were performed on moist surfaces with a standard Knoop MH tester (20 g, 5 s). Data were expressed in Knoop Hardness Numbers (KHN) and analysed by one-way Anova and SNK multiple comparisons (P<0.05). Results: Dentin KHN decreased after acid etching, regardless of etching time. NaOCl treatment after acid etching lowered MH. Conclusions: Treating dentin with either H3PO4 and/or NaOCl caused marked reduction of its surface hardness. Acknowledgements: CICYT/FEDER MAT2004-06872-C03-02.
Dentin Treatment | Microhardness |
Polished | 65.71 (5.2) a |
Phosphoric 7s | 23.89 (10.9) b |
Phosphoric 15s | 21.86 (8.6) b |
Phosphoric 7s + NaOCl | 15.03 (1.4) c |
Phosphoric 15s + NaOCl | 15.30 (2.6) c |