Objective: To determine the resin-dentin bond resistance to degradation of two adhesive systems after the addition of ascorbic acid (AA) on their formulation. Methods: Flat dentin surfaces from forty-eight human molars were bonded according to manufacturer's instructions with an etch-and-rinse (Single Bond-SB) and a self-etch (Clearfil SE Bond-CSE) adhesive system: 1) with the original manufacturer's composition; 2) after addition of 10% AA on the primer/resin formulation. Bonded specimens were sectioned into 1.0 mm2 beams and tested after 24h, after immersion in 10% NaOCl for 5 h, and after 1 or 4 years storing in distilled water. Beams were tensioned at 0.5 mm/min. Results were analyzed by ANOVA and SNK tests (P<0.05). Debonded surfaces were observed by SEM. Results: Mean microtensile bond strength (MTBS) and standard deviations are listed (MPa). Letters indicate differences in columns and numbers in rows.
| 24h water | 5h 10% NaOCl | 1 year water | 4 year water |
Single Bond | 52.4 (8.4) a1 | 24.2 (7.5) b2 | 39.7 (5.7) b3 | 37.4 (10.3) a3 |
Clearfil SE Bond | 39.9 (7.6) b1 | 15.7 (3.1) c2 | 39.5 (7.1) b1 | 28.2 (6.7) b3 |
Single Bond+AA | 44.7 (8.7) b1 | 35.1 (8.1) a2 | 48.3 (7.3) a1 | 29.8 (11.0) b2 |
Clearfil SE Bond+AA | 34.2 (10.6) c1 | 23.5 (6.2) b2 | 23.3 (8.0) c2 | 12.4 (6.0) c3 |