IADR Abstract Archives

Comparison of Contemporary Self-Adhesive Luting Composites

Objectives: High shear-bond-strength (SBS)-values and tolerance to different bonding conditions and materials are essential for the clinical success of self-adhesive luting-materials. Therefore, full functionality after extreme test conditions is a big advantage. In the following study, the focus was on SBS on dentin with blot-dry-(bd) and wet-technique of different self-adhesive luting-materials (translucent shades) compared to Speedcem Plus, both at self- and dual-cure-mode (SC/DC) and before and after thermocycling (TC).
Methods: The following luting composites were employed: SpeedCEM Plus/Ivoclar Vivadent (SCP), G-CEM LinkAce/GC (GCL), Maxcem Elite/Kerr (MCE), PermaCem 2.0/DMG (PC2), SmartCem 2/Dentsply (SC2), RelyX Unicem 2 Automix/3M (RU2).
SBS was measured on bovine dentine (according to ISO-DTS 16506,n=8). Polymerized composite cylinders (TetricEvoCeram/Ivoclar Vivadent) were used for all products to adhere at the dentine specimen. The force was measured using an universal-test-machine (Z010/Zwick-Roell), only measurable samples were considered for analysis. TC was performed between 5°C-55°C and 10’000 cycles (dwell time 30sec). Statistical analysis employed ANOVA, Tukey’s, p<0.05.
Results: Of the materials tested, SBS in DC-mode in general and with wet-technique in special resulted in higher values by trend, except for SC2(bd) and MCE(wet). At SC-mode only SCP demonstrated good and stable results. At DC-mode SCP, GCL and RU2 exhibited similarly favourable results. SCP showed lowest deviations for SBS between SC- and DC-mode, for both bd- and wet-technique.
Conclusions: The shear-bond-strength of contemporary luting composites was investigated in SC- and DC-mode, with/without thermocylcing and with blot-dry- and wet-technique. The wet-technique generally resulted in higher mechanical properties, except for SC2 in SC-mode. Bond strength was independent of curing mode only for Speedcem Plus. Speedcem Plus was the only luting-material that presented a good and favourable outcome on all modes before and after TC, blot-dry and wet. Within the limits of this investigation and regarding clinical efficacy, Speedcem Plus is considered to provide the best set of properties.
Division: Continental European and Scandinavian Divisions Meeting
Meeting: 2019 Continental European and Scandinavian Divisions Meeting (Madrid, Spain)
Location: Madrid, Spain
Year: 2019
Final Presentation ID: 0329
Abstract Category|Abstract Category(s): Dental Materials 2:Polymer-based Materials
Authors
  • Westphal, Michael  ( Ivoclar Vivadent AG , Schaan , Liechtenstein )
  • Gianasmidis, Alexandros  ( Ivoclar Vivadent AG , Schaan , Liechtenstein )
  • Brot, Andreas  ( Ivoclar Vivadent AG , Schaan , Liechtenstein )
  • Grabenbauer, Barbara  ( Ivoclar Vivadent AG , Schaan , Liechtenstein )
  • Kalberer, Deborah  ( Ivoclar Vivadent AG , Schaan , Liechtenstein )
  • Financial Interest Disclosure: Author and co-authors are employees at the R&D departmant (luting materials) of Ivoclar Vivadent AG, Schaan - Liechtenstein.
    SESSION INFORMATION
    Poster Session
    Dental Materials - Adhesion 2
    Friday, 09/20/2019 , 12:00PM - 01:00PM
    TABLES
    Results
    Materialbd: dentin [MPa]bd: dentin TC [MPa]wet: dentin [MPa]wet: dentin TC [MPa]
    SCP SC11.5±1.2a9.7±1.5a12.5±1.1a12.8±1.4a
    SCP DC9.9±2.0a20.5±2.7a12.9±2.3a15.1±4.0a
    GCL SC1.9±2.7***b- ± -*b7.4±4.5****b10.8± -**b
    GCL DC9.9±1.0a20.0±4.0a14.0±1.2*****a23.6±3.9b
    MCE SC- ± -*c- ± -*b3.2±1.1****c1.6± -**c
    MCE DC5.4±2.2***b2.0± -**b0.4± -**b- ± -*c
    PC2 SC3.5±0.5b0.2± -**b3.8±1.0c1.5±0.4***c
    PC2 DC5.6±1.5b3.9±1.2****b9.0±1.1c7.2±2.2d
    SC2 SC4.8± -**d14.9± -**c1.4± -**d2.0±1.5***c
    SC2 DC- ± -*c- ± -*c2.1±1.0*****d0.9±0.2***e
    RU2 SC- ± -*e- ± -*b- ± -*e- ± -*d
    RU2 DC18.1±4.2d23.2±3.8a21.9±3.0e23.8±4.7b
    *: n=0/8, **: n=1/8, ***: n=3/8, ****: n=4/8, *****: n=7/8
    Different superscript letters denominate significant statistical difference in columns.