IADR Abstract Archives

Effect of Location on Strength and Translucency of Multi-Layered Zirconias

Objectives: To examine how the biaxial flexure strength and the translucency change as a function of height in multilayered dental zirconias
Methods: Ten cylinders with a 14.0 mm diameter (expanded for the shrinkage) from each of three multi-layered zirconia materials: e.max®ZirCAD MT-Multi, e.max®ZirCAD Prime and e.max®ZirCAD Prime were milled using PrograMill PM7 milling unit. Pre-fired cylinders were cut in a Buehler IsoMet 1000 saw to produce the top five layers of 1.6 mm thick specimens to produce 1.2 ± 0.2 mm fired specimens. The un-sintered discs were polished using 800 grit SiC. All discs from each layer were sintered at the same time according to the manufacturer's schedule.
Specimens were measured using a Hunter Lab UltraScanVIS Spectrophotometer with a standardized white background and black background using glycerin. Yxy values were obtained for each disc specimen. Using the Y value from the black background and the white background, the contrast ratio was calculated by CR= Yblack/Ywhite.
The disc specimens were loaded in a piston-on-three ball testing fixture detailed in ISO 6872. They were loaded at a loading rate of 0.5 mm/minute. The strength values were calculated by:
σ = -0.2387 P(X-Y)/b2
where σ is maximum strength (MPa); P is fracture load (N), X and Y are loading constants derived from loading configuration and Poison’s ratio and b is thickness of specimen.
Results: The means and standard deviations at each layer for the biaxial flexure strengths( Table 1) and contrast ratios (Table 2) were analyzed with ANOVA (α≤0.05) and are presented for each material below:
Conclusions: Within the bounds of this study, all of the tested materials had the lowest strength values and highest translucency (lowest CR) in the incisal region (layers 1-2) while having the highest strength values and lowest translucency (highest CR) in the body region (layers 4-5).
Division:
Meeting: 2022 AADOCR/CADR Annual Meeting
Location: Hybrid, Atlanta, Georgia
Year: 2022
Final Presentation ID: 0636
Abstract Category|Abstract Category(s): Dental Materials 1: Ceramic-based Materials
Authors
  • Hill, Thomas  ( Ivoclar Vivadent, Inc. , Amherst , New York , United States )
  • Singhal, Shashikant  ( Ivoclar Vivadent, Inc. , Amherst , New York , United States )
  • Tysowsky, George  ( Ivoclar Vivadent, Inc. , Amherst , New York , United States )
  • Financial Interest Disclosure: I am an employee of Ivoclar Vivadent
    SESSION INFORMATION
    VIRTUAL Interactive Talk Session
    Processing, Sintering & Multi-layer Zirconia
    Friday, 03/25/2022 , 08:00AM - 09:30AM
    TABLES
    Table 1 - Biaxial Flexure Strength
    Biaxial Flexure Strength (MPa)
    LayerMT MultiPrimePrime Esthetic
    1786±69
    814±85
    770±119
    2767±74
    961±108
    936±78
    3880±157
    1113±149
    954±85
    4948±73
    1171±161
    1028±165
    4966±53
    1258±173
    1000±156

    Translucency - Contrast Ratio
    Translucency - Contrast Ratio
    LayerMT Multi
    Prime
    Prime Esthetic
    10.583±0.007
    0.553±0.006
    0.542±0.017
    20.599±0.023
    0.608±0.004
    0.577±0.009
    30.669±0.026
    0.686±0.017
    0.645±0.005
    40.679±0.005
    0.699±0.003
    0.646±0.040
    50.667±0.011
    0.710±0.009
    0.688±0.002