IADR Abstract Archives

Impact of fast sintering on material properties of translucent zirconia

Objectives:  Short sintering cycles enable high productivity and flexibility during processing zirconia dental restorations. In this study clinically relevant properties of a translucent zirconia material processed with standard sintering cycle and fast sintering cycle have been compared.

Methods: A translucent zirconia material (Lava Plus, 3M ESPE) was sintered (Lava Furnace 200) with standard sintering protocol 1450°C for 2h dwell time and a faster sintering cycle at 1500°C for 30 min dwell time . Biaxial fracture strength, contrast ratio and color match were analyzed for both sintering cycles. Initial strength was determined according ISO 6872 in a punch-on-three-balls test mode (discs thickness 1.2 mm, diameter 14mm) for n = 30 each group. Contrast ratio respectively opacity was investigated on 1.0 mm polished discs (n=6) with spectrophotometer (Color i7, X-Rite) in remission mode. Color match was investigated visually with three different operators at five different shaded (Lava Plus dying liquids) standardized anterior crowns (n = 3) and compared to each other in a light cabinet (D65, Spectralight lll, X-Rite). Data were analyzed with one-way ANOVA and Tukey's t-test (p<0.05).

Results: Total sintering time, mean fracture strength, contrast ratio and color match results are summarized in following table. 

Standard sintering cylce

Speed sintering cylce

Sintering time without cooling (min)

225

90

Mean fracture strength (MPa)

1160±159

1127±135

Contrast ratio (%)

66.4±0.3

66.6±0.1

Color match

No visible difference

Conclusions: The speed sintering cycle allows a time reduction of more than 2h compared to the standard sintering cycle. No statistical significant difference in fracture strength, contrast ratio and color match was observed between groups sintered with standard and speed sintering cycle. The investigated speed sintering cycle has no impact on clinical relevant material properties of Lava Plus zirconia.


Division: AADR/CADR Annual Meeting
Meeting: 2014 AADR/CADR Annual Meeting (Charlotte, North Carolina)
Location: Charlotte, North Carolina
Year: 2014
Final Presentation ID: 1452
Abstract Category|Abstract Category(s): Dental Materials 3: Ceramic-based Materials and Cements
Authors
  • Herrmann, Andreas  ( 3M ESPE Dental Products, Seefeld, , Germany )
  • Dittmann, Rainer  ( 3M ESPE Dental Products, Seefeld, , Germany )
  • Schechner, Gallus  ( 3M ESPE Dental Products, Seefeld, , Germany )
  • Hauptmann, Holger  ( 3M Deutschland GmbH, Seefeld, , Germany )
  • Popp, Eva  ( 3M Deutschland GmbH, Seefeld, , Germany )
  • Rolf, Jacqueline  ( 3M ESPE Dental Products, St. Paul, MN, USA )
  • Russell, Victoria A.  ( 3M ESPE Dental Products, St. Paul, MN, USA )
  • SESSION INFORMATION
    Poster Session
    Dental Material Properties
    03/22/2014