IADR Abstract Archives

Correlation Between Composite %Filler and Strength, Modulus, and Shrinkage Stress

Objectives: Filler content in composite is credited for increasing strength and reducing shrinkage stress of resin composite. This study evaluated the correlation between the filler percentage and strength, modulus, and shrinkage stress of commercially available flowable and packable dental composites.
Methods: Twenty composites were included in the study (see table). Filler percentage by weight (n=5) was determined through the burned ash technique (800°C for 15 minutes). Three-point bend flexural strength and modulus (n=10) were measured according to ISO 4049 with 2x2x25mm bars, with a cross head speed of 0.75mm/min until fracture. Shrinkage stress (n=8) was evaluated using a universal testing machine in which composite was polymerized through two transparent acrylic rods (diameter = 6.45mm) with a controlled distance 2mm. A Teflon cylinder was placed around the rods to contain the flowable resin composites. The maximum force following 500 seconds of measurement was divided by the surface area of the rod to determine shrinkage stress. Linear correlation between mean filler wt% and flexural strength, modulus, and shrinkage stress were measured by Pearson’s correlation coefficient using SPSS.
Results: The mean +/-standard deviation of the filler wt%, flexural strength, modulus and shrinkage stress are presented in the attached table. There is a positive linear correlation between filler wt% and both flexural strength (r=0.70 p<.01) and modulus (r=0.85 p<0.01) but not shrinkage stress (r=-0.14 p=0.54).
Conclusions: Filler wt% is a good indicator of the stiffness (modulus) and flexural strength of a resin composite. Shrinkage stress may not be determined solely based on filler wt%.
Division:
Meeting: 2024 IADR/AADOCR/CADR General Session (New Orleans, Louisiana)
Location: New Orleans, Louisiana
Year: 2024
Final Presentation ID: 0480
Abstract Category|Abstract Category(s): Dental Materials 2: Polymer-based Materials
Authors
  • Lopez, Carolina  ( UAB School of Dentistry , Birmingham , Alabama , United States )
  • Lawson, Nathaniel  ( UAB School of Dentistry , Birmingham , Alabama , United States )
  • Machado, Nadia  ( UAB School of Dentistry , Birmingham , Alabama , United States )
  • Gomes, Taillk  ( UAB School of Dentistry , Birmingham , Alabama , United States )
  • Lawson, Thomas  ( UAB School of Dentistry , Birmingham , Alabama , United States )
  • Vadapalli, Jayamallika  ( UAB College of Arts and Science , Birmingham , Alabama , United States )
  • Financial Interest Disclosure: Dr Lawson has or has had grants with 3M, Ivoclar, Clinicians Choice, Voco, GC, Kuraray, Kerr, and Dentsply. He has received honorariums from 3M, Ivoclar, Clinicians Choice, GC, Kuraray, Kerr, and Dentsply.
    SESSION INFORMATION
    Poster Session
    Mechanical Properties II
    Thursday, 03/14/2024 , 11:00AM - 12:15PM
    TABLES
    Table1. Results
    COMPOSITEFiller Wt%Flexural strength (MPa)Modulus (MPa)Shrinkage stress (2mm) (MPa)
    Filtek Supreme Ultra Flow
    (3M, USA)
    53.82 +/-1.88127.58 +/-12.856288 +/-3711.88 +/-0.14
    Tetric Evoflow
    (Ivoclar Vivadent)
    52.78 +/-2.2101.03 +/-8.733129 +/-2251.8 +/-0.13
    TPH Spectra ST Flow
    (Dentsply, USA)
    56.9 +/-2.57104.06 +/-9.164435 +/-2391.83 +/-0.22
    Omnichroma Flow
    (Tokuyama, Japan)
    56.68 +/-2.88120.29 +/-6.675301 +/-2761.68 +/-0.09
    Evanesce Flow
    (Clinicians choice)
    52.72 +/-0.6681.95 +/-8.772773 +/-3781.22 +/-0.14
    GrandioSo Flow
    (Voco, Germany)
    77.58 +/-1.31144.23 +/-15.739718 +/-6961.85 +/-0.11
    Gaenial Universal Injectable
    (GC, Japan)
    56.3 +/-3.48107.65 +/-17.235068 +/-2792.01 +/-0.14
    Clearfil Majesty Flow
    (Kuraray, Noritake)
    73.18 +/-3.12143.69 +/-7.278258 +/-8781.94 +/-0.19
    Filtek Bulk Fill Flowable Restorative
    (3M, USA)
    60.57 +/-1.84123.91 +/-20.794263 +/-2421.54 +/-0.10
    Tetric Powerflow
    (Ivoclar Vivadent)
    67.58 +/-1.02100.01 +/-3.835850 +/-4991.7 +/-0.13
    Surefil SDR flow+
    (Dentsply, USA)
    67.49 +/-2.69107.96 +/-10.984790 +/-3181.49 +/-0.12
    Omnichroma Bulk Flow
    (Tokuyama, Japan)
    53.74 +/-3.69124.15 +/-16.025444 +/-4221.82 +/-0.22
    Simplishade Bulk Fill Flow
    (Kerr, USA)
    56.9 +/-1.33107.98 +/-6.545020 +/-4431.41 +/-0.05
    Filtek Supreme Ultra
    (3M, USA)
    71.95 +/-1.21158.76 +/-14.7613188 +/-6311.32 +/-0.11
    Tetric Evoceram
    (Ivoclar Vivadent)
    71.53 +/-2.1102.41 +/-2.736658 +/-5031.67 +/-0.13
    TPH Spectra ST
    (Dentsply, USA)
    67.77 +/-2.4117.45 +/-11.87055 +/-4881.92 +/-0.12
    Omnichroma
    (Tokuyama, Japan)
    65.59 +/-5.81105.42 +/-4.45902 +/-5481.63 +/-0.21
    Harmonize
    (Kerr, USA)
    68.9 +/-1.84115.84 +/-4.118026 +/-5411.81 +/-0.10
    Evanesce
    (Clinicians choice)
    70.34 +/-1.8115.62 +/-12.966669 +/-6261.24 +/-0.16
    GrandioSo
    (Voco, Germany)
    83.52 +/-0.97160.38 +/-19.2614256 +/-10961.6 +/-0.10
    Mean and standard deviation of Filler Wt%, Flexural strength, Modulus and Shrinkage Stress, for all twenty composites included in the study