IADR Abstract Archives

Chemical,structural and mechanical characterization of 4 formulations of composite resin

Objective: Characterization of chemical, structural and mechanical of 4 formulations of composite resin

Method: 48 cylinders of 38,465 mm3 of composite resins were made with the incremental technique using a halogen lamp Astralis3(Ivoclar/Vivadent®). Each specimen was made the test of resistance in compression using a Universal Shimadzu AGS-J test machine. These specimens were grouped as follows: G1:ROK posterior composite(SDI®), G2:FiltekZ-250(3MESPE®), G3:ICE universal composite(SDI®), G4:TetricCeramHR(Ivoclar/Vivadent®). Subsequently, 8 specimens were produced to be analyzed through a DiffractingXRays(XRD) and obtain its crystalline structure.Also,8 Specimens were made to obtain the chemical and morphological analysis through the scanning electronic microscope(2500HITACHI)

Result:  

Level p=0.000 with significant differences. Mean and standard deviation (SD±) expressed in Mpa G1:77,2001(10,1522),G2:95,9617(15,8017),G3:82,1331 (8,71107),G4:71, 9225 (8,37925). The XRD patterns for G2 and G4 showed that they are highly crystalline. G1 and G3 are amorphous. G2 contain yttrium oxide and zirconia; XRD indicates that G4 contains ytterbium fluoride while SEM showed, additionally, crystals of barium aluminum fluorosilicate and quartz. The particle sizes from SEM were:G1:10-25μm,G2:0.01-3.5μm,G3:0.04-0.07μm and clusters <3-5μm,G4:0.04-3.0μm.

Conclusion:

G1 resin has a low value to the traccional resistance, and has an amorphous structure; it means greater concentration of polymers. The G2 while it is the most rigid, this is because it has a crystalline structure that is why it doesn’t stand high concentration of stress. The G3 and G4 have a similar value despite the fact that the G3 has an amorphous structure while the G4 is crystal clear, in fact the most crystal clear from all the groups studied. The properties of the composite resin will depend on the type of organic matrix, the integrity of the coupling silanico between the organic matrix and inorganic filler, of the type, the percentage of particles of filling and the size of these particles that can influence the resistance of composite resins.

Division: IADR/LAR General Session
Meeting: 2012 IADR/LAR General Session (Iguaçu Falls, Brazil)
Location: Iguaçu Falls, Brazil
Year: 2012
Final Presentation ID: 743
Abstract Category|Abstract Category(s): Dental Materials 6: Polymer-based Materials-Chemistry and Composition
Authors
  • Acevedo, Elmer  ( Universidad Nacional Federico Villarreal, Lima, N/A, Peru )
  • Mora, Karla  ( Universidad de Los Andes, Merida, N/A, Venezuela )
  • Ramnarine, Ramnarine Sanchez  ( Universidad de Los Andes, Mérida, N/A, Venezuela )
  • Cordova, Alejandra  ( Universidad de Los Andes, Merida, N/A, Venezuela )
  • Diaz De Delgado, Graciela  ( Universidad de Los Andes, Mérida, N/A, Venezuela )
  • Contreras, Jines  ( Universidad de Los Andes, Mérida, N/A, Venezuela )
  • Delgado, Jose  ( Universidad de Los Andes, Mérida, N/A, Venezuela )
  • Briceño, Mauro  ( Universidad de Los Andes, Merida, N/A, Venezuela )
  • SESSION INFORMATION
    Poster Session
    Photopolymerization and New Approaches to Dental Resins and Composites
    06/21/2012