IADR Abstract Archives

Three-Point Bending Test Parameters For Dental Materials Evaluation

Objective: Three-point bending testing is routinely employed in studies evaluating dental materials. However, testing designs are not well standardized, making inter-study comparisons difficult. The aim of this study was to assess the effects of different three-point bending test design dimensions used in dental papers and in the ISO standards for determination of elastic modulus (E).

Method: Polyvinyl-siloxane molds with five different dimensions were filled with nanofill composite-resin (Filtek Supreme, 3M-ESPE), covered with a glass slide and photoactivated using a quartz-tungsten halogen light for 40s. The 5 different beam sizes were based on dimensions published or specified in ISO standards. The specimens were tested in three-point bending (n=5) and E was determined. E measurements using Knoop microhardness were carried out as control (n=5). Data were analyzed using one-way ANOVA, Tukey’s and Dunnett’s tests (p<.05). Three-dimensional models of the experimentally tested specimens and supports were generated for non-linear finite element analyses (FEA). The materials were assumed as homogeneous, linear-elastic and isotropic. Deflection at the load application point and the maximum tensile stress in the beams were calculated.

Result: Results indicated significant higher E-values with the microhardness method and significant variations between the E-values obtained with the different three-point bending test designs (Table-1). FEA confirmed differences in stress distribution patterns for the different bending test designs evaluated.

Table-1: Elastic modulus for experimental tests.

Composite-resin: Filtek Supreme

Test

E(GPa)±SD

Knoop Microhardness (Control)

17.9±0.3

ISO178 Proportioned (20x2.5x1mm)

10.3±1.0A*

ISO4049 (25x2x2mm)

8.6±0.7B*

Yap & Teoh (12x2x2mm)

3.9±0.1D*

Boaro et al. (12x2x1mm)

7.5±0.8BC*

Pick et al. (10x1x1mm)

6.8±0.4C*

Letters indicate significant difference between rows; *Indicates significant difference between control and experimental groups (p<.05).

Conclusion: Significant different E-values were obtained using the same test-type with different parameters. These discrepancies can lead to complications when using mechanical properties from the literature in inter-study comparisons or finite element stress analyses.

IADR/LAR General Session
2012 IADR/LAR General Session (Iguaçu Falls, Brazil)
Iguaçu Falls, Brazil
2012
2748
Dental Materials 7: Polymer-based Materials-Physical Properties and Performance
  • Raposo, Luís  ( State University of Campinas, Piracicaba, N/A, Brazil )
  • Barreto, Bruno Cf  ( Universidade Federal de Uberlândia, Uberlândia, N/A, Brazil )
  • Sousa, Silas Junior  ( Universidade Federal de Uberlândia, Uberlândia, N/A, Brazil )
  • Pereira, Analice  ( Universidade Federal de Uberlândia, Uberlândia, N/A, Brazil )
  • Costa, Ana  ( State University of Campinas, Piracicaba - SP, N/A, Brazil )
  • Versluis, Antheunis  ( University of Tennessee Health Science Center, Memphis, TN, USA )
  • Correr-sobrinho, Lourenço  ( Piracicaba Dental School, State University of Campinas - UNICAMP, Piracicaba, N/A, Brazil )
  • Soares, Carlos  ( Universidade Federal de Uberlândia, Uberlândia, N/A, Brazil )
  • Poster Session
    Mechanical Testing of Resin-Composites
    06/22/2012