IADR Abstract Archives

Evaluation of Newly Developed PMMA Based Adhesive Resin Cement

Objectives: We have developed the PMMA based adhesive resin cement, called TOKUYAMA MULTIBONDII (MBII). It consists of one liquid based on MMA, two shade powders based on PMMA and one bottle self-etching primer. The borate derivative is used as the chemical polymerization initiator system in MBII. The purpose of this study was to evaluate the tensile bond strength (TBS), tenacity and color change of MBII.

Methods: MBII, TOKUYAMA M-bond (TMB) (Tokuyama Dental Corp.) and C&B-Metabond (CBM) (Sun Medical) were used in this study. TBS; the surfaces of bovine dentin (n=8) were ground (600-grit), bonded to stainless steel rods according to manufacturers' instructions, stored in distilled water (37°C, 24hours), thermo-cycled (10,000 times, between 4°C and 60°C). TBS was measured using a universal testing machine (UTM) (cross-head speed 2.0mm/min). Flexural tests; each cement was cured in the Teflon mold (25mm x 2mm x 2mm) (37°C, 60min), stored in distilled water (37°C, 24hours), polished (1500-grit). Energy (tenacity) at the breaking point or 5.5mm displacement was calculated by three point flexural tests using a UTM (cross-head speed of 1.0mm/min). Color change (Δ b*) of cured cement stored in distilled water (37°C, one year) was analyzed using automatic color analyzer.

Results: After 10,000 thermo-cycles, TBS using MBII, TBM and CBM were 19.1±3.5MPa, 16.0±3.0MPa and 12.9±3.9MPa respectively. Energy of MBII and CBM at 5.5mm displacement was 96.6±4.6mJ and 77.6±4.0mJ respectively and those of TMB at the breaking point was 5.7±1.2mJ. Δ b* of MBII, TMB and CBM were 2.3, 10.3 and 0.5 respectively.

Conclusion: Because of the chemical polymerization initiator system (borate derivative), TBS, tenacity and color of MBII were satisfactory.


Division: IADR/AADR/CADR General Session
Meeting: 2009 IADR/AADR/CADR General Session (Miami, Florida)
Location: Miami, Florida
Year: 2009
Final Presentation ID: 1026
Abstract Category|Abstract Category(s): Dental Materials 6: Polymer-based Materials-Chemistry and Composition
Authors
  • Hirata, Kouichirou  ( Tokuyama Dental Corporation, Tsukuba-city, N/A, Japan )
  • Hamasuna, Y  ( Tokuyama Dental Corporation, Tsukuba-city, N/A, Japan )
  • Kimura, M  ( Tokuyama Dental Corporation, Tsukuba-city, N/A, Japan )
  • Kazama, H  ( Tokuyama Dental Corporation, Tsukuba-city, N/A, Japan )
  • SESSION INFORMATION
    Poster Session
    Dental Polymers Poster I
    04/02/2009