IADR Abstract Archives

Exothermic Heat of Polymerization of Light-cured and Self-cured Core Materials

Objectives: To measure the total energy per gram released and the maximum temperature reached during the polymerization of composite core materials, using differential scanning calorimetry (DSC).

Methods: Four core buildup materials, two light cured (LC), Getz blue core (Teledyne Waterpik Ft Collins CO), Light-Core (Bisco Inc Schaumburg IL) and two self cure composites (SC) Compcore AF (Premier , Plymouth meeting PA) Bis-Core (Bisco) were measured in a DSC6 (Perkin Elmer Instruments Norwalk CT).

The LC materials were exposed to 400mW/cm2 for 30 sec intervals. The energy of the light source was subtracted from the initial energy released to obtain the exothermic energy. The SC materials were mixed for 1 minute, weighed and placed in the DSC. The released energy DH and the peak temperature were recorded. All measurements were isothermal at 35°C. Five specimens were made for each group, of about 100 mg each.

Results: See table below. (* and # indicate the two groups that are different at p<0.05)

Conclusions: The LC systems reached the highest temperature during the curing cycle. The heat of polymerization does vary considerably for these materials


Division: AADR/CADR Annual Meeting
Meeting: 2003 AADR/CADR Annual Meeting (San Antonio, Texas)
Location: San Antonio, Texas
Year: 2003
Final Presentation ID: 818
Abstract Category|Abstract Category(s): Dental Materials: V - Polymer Materials-Chemistry
Authors
  • De Rijk, Wademar G.  ( University of Tennessee, Memphis, TN, USA )
  • Lackey, Mark  ( Unversity of Tennessee Memphis, Memphis, TN, USA )
  • SESSION INFORMATION
    Oral
    Materials Structure/Properties/Conversion
    03/14/2003