Assessment of Dentin-resin Cement Interface after Acid-base Challenge
Objectives: The purpose of this study was to evaluate dentin bond strength and to observe the adhesive-dentin interface after acid-base challenge using three different adhesive resin cements. Methods: CAD/CAM resin blocks (Estelite Block, Tokuyama Dental) were cut into slices of approximately 2 mm thickness. Thirty dentin surfaces from caries-free human premolars were ground and bonded to CRB with using one of three dual-cure resin cements: PANAVIA V5 (V5, Kuraray Noritake Dental), ESTECEM II (E II, Tokuyama Dental) or Rely X Ultimate (RXU, 3M ESPE) according to the manufacturer’s instruction. A microtensile bond strength (μ TBS) test was undertaken with 0, 5000 and 10,000 thermal cycles, and the interface of the bonded specimens after acid-base challenge was examined by SEM. μ TBS were statistically analyzed using 2-way ANOVA and t-test with Bonferroni correction at α=0.05. Results: The μTBS of V5 exhibited a stable bond strength despite thermal cycling while the bond of EII and RXU after 10,000 cycles dropped significantly among all thermal cycle periods (p <0.05). An acid-base resistant zone (ABRZ) was observed in all groups, however, the morphology of the bonded interface differed among the tested cements. Conclusions: V5 provided most reliable bonding performance to dentin of human premolars and presented durability against acid-base challenge.
Division: IADR/AADR/CADR General Session
Meeting:2019 IADR/AADR/CADR General Session (Vancouver, BC, Canada) Location: Vancouver, BC, Canada
Year: 2019 Final Presentation ID:0691 Abstract Category|Abstract Category(s):Dental Materials 4: Adhesion
Authors
Aung, San San May Phyo
( Tokyo Medical and Dental University
, Tokyo
, Bunkyo-ku
, Japan
)
Takagaki, Tomohiro
( Tokyo Medical and Dental University
, Tokyo
, Bunkyo-ku
, Japan
)
Ko Ko, Aye
( Tokyo Medical and Dental University
, Tokyo
, Bunkyo-ku
, Japan
)
Mean values and standard deviations of microtensile bond strength values of all groups
V5
E II
RXU
0 TC
55.1 ± 6.1(10/70/20/0)
61.9 ± 6.3 A, B (10/80/10/0)
49.9 ± 5.5 D, E (20/70/10/0)
5000 TC
55.5 ± 5.1(0/90/10/0)
53.5 ± 5.2 A, C (0/80/20/0)
37.6 ± 6.0 D, F (30/30/40/0)
10000 TC
52.6 ± 4.8(10/60/20/10)
44.7 ± 5.7 B, C (30/20/50/0)
28.8 ± 4.7 E, F (50/30/20/0)
n=10
Data are shown as mean ± standard deviation.
Same large superscript letters indicate statistically significant difference between bond strength (p <0.05).
Percentage of failure mode (Adhesive failure at the resin-dentin interface/ Cohesive failure completely within the resin cement/ Partial adhesive failure, where remnants of resin remained on the dentin surface/ Cohesive failure in the dentin)