IADR Abstract Archives

Shear Bond Strength of RelyX™ Unicem 2 to Dentin in Comparison to Latest Self-Adhesive Resin Cements

Objectives: Recently, several manufacturers have launched new self-adhesive resin cements (SARCs), claiming excellent bond strength to the tooth surface. However, it is still unclear how those SARCs compare to the well-established self-adhesive resin cement RelyX™ Unicem 2 in terms of shear bond strength (SBS) to the challenging substrate dentin. Therefore, this study determined SBS to dentin of RelyX™ Unicem 2 and latest self-adhesive resin cements before and after artificial aging.
Methods: Breeze® Self-Adhesive Resin Cement (BSARC, Pentron), Calibra® Universal (CU, Dentsply), G-CEM LinkAce™ (GCLA, GC), Maxcem Elite™ Chroma (MEC, Kerr), Panavia™ SA Cement Plus (PSAC+, Kuraray), PermaCem 2.0 (PC2, DMG), RelyX™ Unicem 2 Automix (RXU2, 3M ESPE) and SpeedCem® Plus (SCP, Ivoclar) were tested. All cements were used according to manufacturers’ instructions. Bovine teeth were ground flat to expose dentin, polished (grit 320 sandpaper), water-rinsed, and gently air-dried. Stainless steel rods (diameter=4mm) were sandpapered, sandblasted, silanized (ESPE™ Sil, 3M ESPE) and subsequently cemented (n=6) under standardized pressure (20g/mm2). For self-curing, glycerine gel (Airblock™, Dentsply™) was applied. For light-curing, the cement was irradiated from 4 sides (10s each; Elipar™ S10, 3M ESPE). The specimens were stored for 1h under pressure (36°C) followed by additional 24h (36°C; 100% relative humidity) without pressure. Part of the specimens was subjected to artificial aging (thermocycling: 5000 cycles, 5°C-55°C) before shear bond strength (SBS) testing (Zwick Z010; n=6; speed=0.75mm/min). Data analysis was performed using One-Way ANOVA (Tukey; p<0.05).
Results: See table.
Conclusions: The well-established self-adhesive resin cement RelyX™ Unicem 2 is always in the statistical group with the best adhesion performance to dentin under all testing conditions. Specifically, adhesion performance of RelyX™ Unicem 2 was not negatively affected by artificial aging in contrast to some competitive self-adhesive resin cements.
IADR/PER General Session
2018 IADR/PER General Session (London, England)
London, England
2018
0935
Dental Materials 4: Adhesion
  • Claussen, Kai  ( 3M Deutschland GmbH , Seefeld , Germany )
  • Ludsteck, Manfred  ( 3M Deutschland GmbH , Seefeld , Germany )
  • Hader, Sigrid  ( 3M Deutschland GmbH , Seefeld , Germany )
  • Hecht, Reinhold  ( 3M Deutschland GmbH , Seefeld , Germany )
  • All authors are employed by 3M Deutschland GmbH and thus have financial interest in this abstract.
    Poster Session
    Self-adhesive and Bioactive Bonding Materials
    Thursday, 07/26/2018 , 11:30AM - 12:45PM
    Shear bond strength (SBS) of self-adhesive resin cements with standard deviation (STD) before and after thermocycling (TC). Means that do not share the same letter in a column are significantly different.
    CementSBS to Dentin sc
    [MPa] ± STD
    SBS to Dentin lc
    [MPa] ± STD
    SBS to Dentin sc after TC
    [MPa] ± STD
    SBS to Dentin lc after TC
    [MPa] ± STD
    BSARC5.3 ± 1.0 A,B17.0 ± 2.9 A3.8 ± 4.4 A,B15.3 ± 2.9 A
    CU7.0 ± 1.6 A,B7.5 ± 2.9 B,C5.6 ± 2.2 A,B7.5 ± 3.1 A,B
    GCLA7.9 ± 2.7 A,B10.1 ± 5.4 A,B,C10.1 ± 4.0 A8.8 ± 4.6 A,B
    MEC3.6 ± 1.3 B3.7 ± 1.5 C1.9 ± 1.3 B4.3 ± 4.7 B
    PSAC+8.1 ± 2.8 A,B16.6 ± 4.4 A10.0 ± 3.3 A9.0 ± 5.9 A,B
    PC26.3 ± 2.7 A,B8.8 ± 0.2 A,B,C9.4 ± 3.4 A0.9 ± 1.0 B
    RXU27.7 ± 2.0 A,B15.2 ± 3.5 A,B10.1 ± 3.9 A13.8 ± 4.3 A
    SCP9.6 ± 4.6 A17.4 ± 8.9 A7.0 ± 5.0 A,B8.1 ± 2.2 A,B