IADR Abstract Archives

Evaluation of Different Ceramic Pretreatments Using a New Universal Adhesive

Objectives: Dependent from the application silicate-ceramics requires different ceramic pretreatments. When luting indirect restorations it is recommended to etch extraorally the surface with hydrofluoric acid prior silanisation. The intraoral usage of hydrofluoric acid is not riskless. Therefore other ceramic pretreatments are necessary when repairing indirect restorations intraorally.
The aim of this study is to investigate the effects of different ceramic pretreatments prior application of the new Universal Adhesive (IBUN, Heraeus Kulzer) on the shear bond strength (SBS) to Venus Diamond (A2, Heraeus Kulzer).

Methods: As ceramic substrate HeraCeram Sun (Heraeus Kulzer) was used. As adhesive iBUN + Ceramic Primer (CP, Heraeus Kulzer) was used. The ceramic surface was sandblasted using Al2O3 (50µm) or glass beads (Bego Perlablast, 50µm, DIN 8201) with 1.5bar pressure before adhesive application. Grinding was done either with SiC-paper 320grid (P400) or a K1 grinder. For cleaning HF (9 %, Porcelain Etch, Ultradent) or H3PO4 (Etch 35 Gel, Heraeus Kulzer) was used. After each step the ceramic surface was rinsed with water for 20s. Bonding was performed either with or without iBCP (10s setting time + air-drying) prior the iBUN treatment. Shear bond strength (SBS) was measured according ISO 29022 after thermo-cycling (5000 cycles, 5-55°C/10s dwell time).

Results: Results are shown in the table.
Conclusions: The results showed that shear bond strength to ceramic is influenced by the preconditioning process.

Division: IADR/AADR/CADR General Session
Meeting: 2015 IADR/AADR/CADR General Session (Boston, Massachusetts)
Location: Boston, Massachusetts
Year: 2015
Final Presentation ID: 2286
Abstract Category|Abstract Category(s): Dental Materials 1: Adhesion - Bond Strength Testing and Mechanisms
Authors
  • Schaub, Matthias  ( Heraeus Kulzer GmbH , Hanau , Germany )
  • Kastrati, Astrit  ( Heraeus Kulzer GmbH , Hanau , Germany )
  • Eppinger, Regina  ( Heraeus Kulzer GmbH , Hanau , Germany )
  • Loh, Waltraut  ( Heraeus Kulzer GmbH , Hanau , Germany )
  • Leyer, Andrea  ( Heraeus Kulzer GmbH , Hanau , Germany )
  • Schweppe, Janine  ( Heraeus Kulzer GmbH , Hanau , Germany )
  • Support Funding Agency/Grant Number: Heraeus Kulzer GmbH
    Financial Interest Disclosure: I am employee of Heraeus Kulzer.
    SESSION INFORMATION
    Poster Session
    Universal Adhesives
    Friday, 03/13/2015 , 03:30PM - 04:45PM
    TABLES
    SBS of different ceramic pretreatments
    CP SBS [Mean/SD in MPa]
    Extraoral pretreatment of ceramic
    Al2O3 - + 12.9±2.0
    Al2O3 20s H3PO4 + 30.0±8.8
    Glass beads - + 29.1±2.6
    Al2O3 90s HF - 19.6±2.5
    Al2O3 90s HF + 21.0±6.4
    Intraoral pretreatment of ceramic
    SiC-Paper - + 32.1±2.1
    K1-grinder - + 28.2±4.3
    SiC-Paper 20s H3PO4 + 32.6±4.5
    SiC-Paper 90s HF - 8.5±1.0
    SiC-Paper 90s HF + 15.5±3.7