IADR Abstract Archives

Effect of polymerization technique of resin cement on void formation

Objective: Little is known about the density of the dual-cure cements when polymerized by different techniques of immediate light-cure or chemical-cure (5- minutes) prior to light-curing.  This study is to determine if there is a difference in number and size of porosities in dual-cure cements depending on the polymerization technique.

Method: Forty identical composite block tooth replicates of molar MOD-onlay preparations were fabricated.  A standardized three-surface Empress CAD (Ivoclar Vivadent Liechtenstein) porcelain onlay was designed and manufactured utilizing Cerec-3D (Sirona Dental Systems,NC.USA) and replicated forty times. Bonding surfaces of porcelain were etched with hydrofluoric acid and silinated.  Onlays were randomly cemented with one of two cements Multi-Link (Ivoclar)-(M) and Relyx (3M) St Paul MN, USA)-(R) and immediately polymerized (I) for 20-seconds with a Valo (Ultradent S.Jordan,UT.USA) or allowed to autopolymerize-(A) for five minutes followed by a 20-second light-cure.   Ten specimens each MI, MA, RI and RA were cemented-polymerized.  Specimens were stored for a minimum of two-weeks prior to 3D microCT (at 100uA) analysis performed with Bruker Skyscan1172 (Madison,WI.USA).  MicroCT images were individually reconstructed/analyzed for the presence of voids and software reassembled to determine the volume and number of voids utilizing NRECON and CTAn (Skyscan).  Mean void size and percent voids calculated and ANOVA utilized to evaluate significant difference.

Result: Mean number of voids(+s.d.): RI 150(+46), RA 55(+25), MI 7(+8), MA 23(+26) and percent voids(+s.d.) RI 46(+14), RA 52(+11), MI 1.3(+1.4), MA 1.5(+1.0) were calculated for significant differences.  Relyx had significantly greater numbers and percent voids than Multi-Link (p<0.01).

Conclusion: Multi-Link showed no difference in number or percentage of voids between the immediate light-curing and chemical-cure followed by light-cure.  Relyx chemical-cure followed by light-cure demonstrated smaller size, number, and percentage of voids than immediate light-cure.  Size, number, and percent of voids may influence bond strength and performance and require further investigation.

Division: IADR/AMER General Session
Meeting: 2014 IADR/AMER General Session (Cape Town, South Africa)
Location: Cape Town, South Africa
Year: 2014
Final Presentation ID: 153
Abstract Category|Abstract Category(s): Dental Materials 7: Polymer-based Materials-Physical Properties and Performance
Authors
  • Wolff, Samantha  ( New York University College of Dentistry, New York, NY, USA )
  • Estafan, Denise  ( New York University College of Dentistry, New York, NY, USA )
  • Saebo, Karen  ( New York University College of Dentistry, New York, NY, USA )
  • Wolff, Mark  ( New York University, New York, NY, USA )
  • SESSION INFORMATION
    Oral Session
    Keynote Address; Resin Cements and Aesthetic Dental Materials
    06/26/2014