IADR Abstract Archives

Mechanical characterization of short fiber reinforced composite Xenius

Objective: Short fiber reinforced filling composite (Xenius Base) is a new type filling composite which is designed to dental application that needs high toughness properties, like for base structure for large restorations or partial crowns.
The aim of this study was to find correlation of the composite crown fatigue load to various biomechanical properties eg. fracture toughness, flexural- , compression-  and diametral tensile test.

Method: Specimens (n=10/gr) were fabricated either Xenius Base (Sticktech) or restorative composite (G-ænial Anterior, GC). Specimens for all tests were prepared using layering technique with light polymerization (Elipar S10, 3M ESPE) for 40 sec. Flexural test were prepared according to ISO 4049 (size 2x2x25mm), compression- and diametral tensile strength according to ISO 4104 (ø 4.0 mm, 6 mm height) and single-edge notched-bend fracture toughness Kic adapted ISO 20795-2 (2x2x25mm). Fatigued load of anterior composite crowns (N=20/gr) were evaluated using a staircase approach with maximum 10000 cycles zirconia-jig tested at water.  All results were statistically analyzed with analysis of variance (ANOVA) and Pearson-correlation. 
Result: XENIUS base revealed high fracture toughness properties, which had strong correlation to fatigue load (r=0,93, p <0.05). Flexural strength and diametral tensile strength had medium correlation, whereas no correlation was found between fatigue load and compression strength.

Material Crown fatigue load (N) Fracture toughness (Kic) Flexural strength (MPa) Diametrial tensile strength (MPa) Compression
strength (MPa)
Anterior  135.0 (63.7) 1.78 (0.16)  86.9 (9.0) 115.8 (13.6) 252.3 (49.1)
XENIUS Base 266.7 (22.5) 4.52 (0.86) 107.3 (14.2) 140.5 (18.6) 238.9 (52.5)

Conclusions: The new short fiber composite show very high fracture toughness properties, which strongly correlated to fatigue load of composite crown. Conventional biomechanical test like flexural test did not reveal good estimate for fatigue properties. This suggests that fracture toughness is proper estimate for durability of restoration for high-load-bearing areas.

Division: IADR/AADR/CADR General Session
Meeting: 2013 IADR/AADR/CADR General Session (Seattle, Washington)
Location: Seattle, Washington
Year: 2013
Final Presentation ID: 1562
Abstract Category|Abstract Category(s): Dental Materials 7: Polymer-based Materials-Physical Properties and Performance
Authors
  • Lassila, Lippo  ( University of Turku,Institute of Dentistry,Department of Biomaterials Science and Turku Clinical Biomaterials Centre-TCBC, Turku, , Finland )
  • Garoushi, Sufyan  ( University of Turku,Institute of Dentistry,Department of Biomaterials Science and Turku Clinical Biomaterials Centre-TCBC, Turku, , Finland )
  • Bijelic, Jasmina  ( University of Turku, Turku, N/A, Finland )
  • Vallittu, Pekka  ( University of Turku, Turku, N/A, Finland )
  • SESSION INFORMATION
    Oral Session
    Characterization of Mechanical Properties
    03/22/2013