IADR Abstract Archives

Bonding Measurements: Strength and Fracture Mechanics Approaches

Objectives: The goal of this study was to test the hypothesis that there was no effect of cross-sectional area on the tensile strength and apparent toughness of monolithic and bilayered dental ceramics using microtensile specimens.

Methods: Zirconia cores (e.max®ZirCAD) were veneered and cut to produce specimens with three different cross-sectional areas: 1.00 mm2; 1.44 mm2; and 2.25 mm2 using heat-pressed glass veneer (e.max®ZirPress). In addition, monolithic glass veneer (e.max®ZirPress) specimens with the same dimensions were also prepared (N=20 each). Bilayered and monolithic specimens were tested in tension until fracture and reported as interfacial bond strength and tensile strength respectively. Furthermore, fracture surface of all specimens were observed under optical and electron microscopes. The apparent toughness of both bonded bilayered and monolithic specimens was calculated from critical cracks and fracture strength. Mean interfacial bond strength, tensile strength, and apparent toughness were analyzed using one-way ANOVA and Tukey HSD (p<0.05).

Results: The results showed that cross-sectional area had effect on interfacial bond strength and tensile strength of bilayered dental ceramic and monolithic glass veneer respectively (Table 1). However, there was no significant difference in the apparent toughness of both bilayered dental ceramic and monolithic glass veneer groups.

Table 1: Tensile strength and apparent toughness (SD in parenthesis) of bilayered and monolithic specimens*

Materials

Tensile strength (MPa)

Apparent toughness (MPa.m1/2)

1 mm2

1.44 mm2

2.25 mm2

1 mm2

1.44 mm2

2.25 mm2

Bilayered

17.6(6.1)A

14.8(5.1)AB

12.0(3.1)B

0.23(0.10

0.21(0.07)

0.19(0.08)

Monolithic

26.9(5.6)a

23.5(5.3)ab

20.4(6.1)b

0.41(0.11)

0.41(0.09)

0.38(0.09)

*The values with the same superscript are not significantly different.

Conclusions: This study demonstrated that cross-sectional area had no effect on apparent toughness of bilayered dental ceramics and monolithic glass veneer. Fracture mechanics approach, using critical crack size and strength, may be more reliable approach for testing bonding quality than bond strength test.

Division: IADR/AADR/CADR General Session
Meeting: 2013 IADR/AADR/CADR General Session (Seattle, Washington)
Location: Seattle, Washington
Year: 2013
Final Presentation ID: 166
Abstract Category|Abstract Category(s): Dental Materials 1: Adhesion - Bond Strength Testing and Mechanisms
Authors
  • Anunmana, Chuchai  ( Mahidol University, Bangkok, N/A, Thailand )
  • Wansom, Wiroj  ( Mahidol University, Bangkok, N/A, Thailand )
  • SESSION INFORMATION
    Oral Session
    Bonding to Dentin; General; Adhesives
    03/20/2013